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    Automatic Derivatization System for Phenethylamine Drugs - Applications

    NEW

    Applicable to GCMS-QP2050, GCMS NX series

    Application to Authentic Samples Using Automatic On-column Derivatization System

    • An authentic urine sample was pretreated using the liquid-liquid extraction shown in Fig. 1. TFA derivatives of methamphetamine and amphetamine were detected in the urine samples. These results demonstrate the ability of qualitative and quantitative analysis using 2-step injection with high selectivity in authentic samples.

    • sample-pretreatment-flow.


      Fig.1 Sample pretreatment flow

    Total Ion Current Chromatograms (TICC) of authentic urine sample
     

    Fig. 2 Total ion current chromatograms (TICC) of authentic urine sample

    Mass Chromatograms of Detected Drugs
     

    Fig. 3 Mass chromatograms of detected drugs