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    SALD-7500nano - Specs

    Nano Particle Size Analyzer

    System Structure

    An evolved nano particle size analyzer for accurate evaluation of nano particles
    Main unit (Measurement unit): SALD-7500nano

    • Violet semiconductor laser (wavelength: 405 nm) is used for the light source. Maintenance, such as gas replacement, is unnecessary.
    • The detector incorporates 78 elements at the front, one element at the side, and 5 elements at the back for a total of 84 elements. Additionally, high-sensitivity light receptors that support violet semiconductor laser wavelengths are adopted with all detectors.
    • The fixed parts of the cell and cell holder can be pulled out at the front of the unit using a slide mechanism. This makes it easy to mount and replace cells, and to perform maintenance.
    • WingSALD ll software is supplied as standard. It offers versatile data processing and simple, high-speed operation to suit every purpose and processing requirement.

    Add optional units to the SALD-7500nano to design a wide range of systems.

    The batch cell and the high-concentration sample measurement system can be set in the measurement unit.
    Small-volume Measurement System (SALD-7500nano and SALD-BC75)
    High-Concentration Sample Measurement System (SALD-7500nano and SALD-HC75)
    Ultra Small-Volume Measurement System (SALD-7500nano and SALD-HC75 and “Glass Slides with Indentation”)

    Easy Measurement under PC Control
    Sampler SALD-MS75

    • Groups of particles are dispersed in a liquid medium and measured as they are circulated between the flow cell, which is placed in the measurement unit, and a dispersion bath in the sampler.
    • The dispersion bath incorporates a stirrer and an ultrasonic sonicator. A pump delivers the dispersed suspension to the flow cell.
    • The pump is specially designed to ensure both liquid medium and the particles are circulated. A stainless ball of 2 mm circulates and it is possible to measure it.
    • It can be controlled from a PC.
    • Most organic solvents can be used as dispersion media.

    Sample Unit SALD-MS75 Solvent Resistance

    Note1

    Solvent resistance toward materials used in the passageways of SALD-MS75. Solvent resistance values are representative, and are not certified.

    Note2

    Only applicable for liquid pump. Not applicable for liquid supply pump.

    Note3

    Ultrasonic cleaning instruments are needed for the measurement of reference sample.

    Measurement data

    Ideal for Measurement with Small Amounts of Organic Solvent
    Batch Cell SALD-BC75

    • Measurement is possible with a small amount of sample (i.e., measured particles) and liquid medium (i.e., dispersion medium).
    • The capacity of the batch cell is only 7cm3 an so waste treatment for the suspension canbe performed with relatively small amounts.
    • The vertical motions of the stirring plate prevent sedimentation of the particles.
    • The funnel reduces the possibility of sample spillage.
    • A tetrafluoroethylene resin funnel is provided to reduce the possibility of suspension getting on the hands of the user. It also prevents the cell surface from becoming dirty.

    Measurement data

    Measurement Samples without Dilution
    High-Concentration Sample Measurement System: SALD-HC75

    • High-concentration samples can be measured using the laser diffraction method.
    • Measurement is possible by simply holding the high-concentration sample particles to be measured between two glass slides.
    • Samples for which the particle size distribution would be changed by dilution can be measured in their original state, or with the minimum required level of dilution, and a true image of the measurement object can be obtained.
    • Commercial hand creams, face creams, and rinses can be measured with hardly any pretreatment.

    If a standard flow cell or batch cell is used to measure a sample at a high concentration, the long light pathlength results in multiple scattering, making it difficult to obtain accurate measurements.
    With this system, however, it is possible to hold the high-concentration sample particles between two glass slides, which shortens the length of the light paths, avoids the negative effects of multiple scattering and makes accurate measurement possible.

    Glass sample plates (glass with indentation) (Option)

    Effective for measuring samples with relatively low concentrations, or expensive samples that can only be used in small amounts.

    Measurement Data

    SALD-7500nano

    General Specifications

    Measurement principle

    Laser Diffraction Method

    Measurement range

    7 nm (0.007 μm) to 800 μm (when using sampler)
    7 nm (0.007 μm) to 400 μm (when using batch cell)
    30 nm (0.03 μm) to 280 μm (when using high-concentration sample unit)

    Note 1: The measurement range varies according to the shape etc. of the particle.

    SALD-7500nano

    Measurement unit

    Light source

    Semiconductor laser (Wavelength 405 nm)

    Light detector

    Detector elements for violet semiconductor laser Total 84 elements
    (78 forward, 1 side, 5 back)

    System Compliance

    Class 1 Laser Product, CE

    Required power supply

    AC 100 V±10%, 1 A, 50/60 Hz

    Dimensions & weight

    Approx. 680 × D280 × H430 mm, Approx.32 kg

    Operation environment

    Temperature : 10 to 30°C , Humidity : 20 to 80% (no condensation)

    Note 2: Reference sample and USB cable (2 m) supplied as standard
    Note 3: Ultrasonic cleaning instruments are needed for the measurement of reference sample.

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    SALD-MS75

    Sampler

    Dispersing bath

    Capacity : 100 / 200 / 300 mL

    Sonicator

    Frequency : about32 kHz, output : about 40 W

    Liquid Pump

    Radial pump, maximum flow rate 2000 cm3/min

    Liquid Pump Material

    Stainless (SUS 304, SUS 316), Tetrafluoroethylene (PTFE),
    Perfluoroelastmor (FEP)

    Liquid Supply Pump

    Diaphragm pump, maximum flow rate : 750cm3/min

    Liquid Supply Pump Material

    Polypropylene

    Flow Cell

    Quartz glass

    Required power supply

    AC 100 V±10%, 2 A, 50/60 Hz

    Dimensions & weight

    Approx. W390 × D520 × H430 mm, Approx.18 kg

    Operating Environment

    Temperature: 10 to 30°C, Humidity: 20 to 80% (no condensation)

    Note 4: USB cable (2 m) supplied as standard

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    SALD-BC75

    Batch Cell

    Cell Material

    Quartz glass

    Required Liquid Volume

    Approx. 5 cm3

    Stirrer Mechanism

    Up-and-down movement of blade

    Dimensions & weight

    Approx. W100 × D120 × H140 mm, Approx. 0.8 kg

    Operating Environment

    Temperature: 10 to 30°C, Humidity: 20 to 80% (no condensation)

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    SALD-HC75

    High-concentration Sample Measurement System

    Cell Material

    Borosilicate glass

    Required Liquid Volume

    Approx. 0.15 cm3

    Dimensions & weight

    Approx. W20 × D100 × H9 mm, Approx. 0.2 kg

    Operating Environment

    Temperature: 10 to 30°C, Humidity: 20 to 80% (no condensation)

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    WingSALD II

    Measurement and Data Display Functions

    Measurement of Particle Size Distribution

    Allows measurements using measurement assistant unction (interactive process based on SOP) and manual mode

    Automatic Calculation of Refractive Index

    Automatic calculation by Light Intensity Distribution Reproduction (LDR) method based on specified substance name or range

    Real-Time Display

    Particle size distribution / Light intensity distribution simultaneous display

    Recalculation of Particle Size Distribution

    Max. 200 data batch calculation or individual data calculation

    Display of Particle Size Distribution Data

    Max. 200 data overlay graph or individual data graph

    Display of Light Intensity Distribution

    Max. 200 data overlay graph or individual data graph

    Diagnostics/Adjustments

    Self-diagnostic functions

    Statistical Data Processing

    Max. 200 data (Max. 200 data overlay graph)

    Time Series Analysis

    Max. 200 data

    3-Dimensional Graph

    Max. 200 data

    Data Transfer via Clipboard

    Image Output, Image Output

    Data Sorting

    Sort by file name, sample ID, sample number, or refractive index.

    Note 5: The Light Intensity Distribution Reproduction (LDR) method calculates the refractive index from the conformity between the measured light intensity distribution pattern and the light intensity distribution data reproduced (calculated) from the particle size distribution data. LDR is a proprietary method developed by Shimadzu. Two papers have been published on this method. It is sometimes called the "Kinoshita Method" at academic conferences.

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    WingSALD II

    Output Conditions

    Particle Size Distribution (μm) Number of Divisions

    Fixed 51 / 101 divisions / Optional (can be set by user) 51 divisions * 10 tables

    Particle Mass Distribution (%) Number of Divisions

    Fixed 51 divisions, Optical (can be set by user) 51 divisions * 10 tables

    Dimension of Particle Amount

    Count, length, area or volume

    Expression of Cumulative Distribution

    Undersize, oversize

    Expression of Data Frequency

    q, q / Δ×, q / Δlog×

    Smoothing Level

    10 Level

    Distribution Function Fitting

    Rosin-Rammler distribution, logarithmic Gaussian distribution

    Data Shifting

    ±10 levels

    Report Functions

    Batch output possible by selecting single data, overlay data, statistical data, time-series data, or 3D data

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    WingSALD II

    Data Analysis

    Scattering Angle Evaluation

    Max. 200 data overlay graph or individual data graph

    Data Conversion Function

    Emulation of particle distribution data by other instruments or measuring principles

    Mixing Simulation Function

    Max. 6 points

    Data Connection Function

    2 data connections

    Continuous Measurements Function

    Measurement interval: 1 s min., Save up to 200 data points

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    SALD-7500nano

    Measurement unit

    Measurement range

    7 nm to 800 µm

    Light source

    Violet semiconductor laser (405 nm wavelength)

    Detection elements

    84 elements

    Options

    Batch cell, multifunction sampler, high-concentration measurement system

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