LC/MS/MS Method Package for Water Quality Analysis

For LabSolutions™ LCMS Software

Ready-to-Use Methods Provided

Shimadzu provides method files, including pre-registered MRM parameters with optimized quantitative and reference ions, LC separation parameters, and retention times and peak identification parameters for each compound, as well as report templates for outputting quantitation results, as a package. If retention times are adjusted when the system is introduced, based on the HPLC configuration delivered, the analysis process can be started as soon as the specified columns, mobile phases, and standard samples are supplied.

Smooth Analysis of Multiple Analytes with LabSolutions Insight

When analyzing data for multiple components and analytes, everything from batch analysis to the creation of reports can be performed by LabSolutions Insight. LabSolutions Insight is a software program equipped with quantitative analysis and screening functions. In the analysis window, information is displayed for each target compound and set of measurement data, and both quantitative values and area values can be listed. This allows the user to select the easiest display method for checking the data in accordance with the workflow. In addition, by using the flagging function, only the results exceeding specified standard values are displayed, improving the analytical throughput of multiple components and analytes subject to the regulations.

Methods Easily Customized

Since LabSolutions Version 5 enables the addition or deletion of components to be analyzed, methods can be easily customized. In addition, the package includes a compound parameter list enables the creation of new tables that list only the components needed.

Compounds List

Golf Course Pesticides: 44 compounds

HPLC Conditions

Analytical column : Shim-pack XR-ODSII (150 mmL. × 2.0 mmI.D., 2.2μm)P/N 228-41623-93
Mobile phase A : 5 mmol / L Ammonium acetate - Water
Mobile phase B : 5 mmol / L Ammonium acetate - Methanol
Flow rate : 0.2 mL / min
Injection volume : 5 μL
Column temperature : 40 °C

Step	Time(min)	A(%)	B(%)
0	0	80	20
1	13	10	90
2	23	10	90
3	23.01	80	20
4	28	80	20

Compound Name

Acetamiprid
Azoxystrobin
Bensulide
Boscalid
Butamifos
Cafenstrole
Cafenstrole metabolite
Clothianidin
Cumyluron
Cyclosulfamron
Cyproconazole
Diazinon
Difenoconazole
Dithiopyr
Ethoxysulfron

Fenitrothion
Flazasulfuron
Flutolanil
Harosulfuron-methyl
Imidacloprid
Iprodione
Isoprothiolane
Isoxathion
Mecoprop
Mepronil
Metalaxyl
Oxaziclomefone
Pencycuron
Pendimethalin
Propiconazole

Propyzamide
Pyributicarb
Siduron
Simazine
Simeconazole
Tebuconazole
Tebufenozide
Terbucarb
Tetraconazol
Thiamethoxam
Thifluzamide
Triclopyr
Triflumizole
Triflumizole metabolite

Pesticides Targeted for Water Quality Control: 32 compounds

HPLC Conditions

Analytical column : L-Column ODS (150 mmL. × 2.1 mmI.D., 5μm)
Mobile phase A : 0.1% formic acid - Water
Mobile phase B : Acetonitrile
Flow rate : 0.2 mL / min
Injection volume : 10 μL
Column temperature : 40 °C

Step	Time(min)	A(%)	B(%)
0	0	100	0
1	30	0	100
2	35	0	100
3	35.01	100	0
4	45	100	0

Compound Name

2,4-D
Asulam
Azoxystrobin
Bensulfuron-methyl
Bensulid(SAP)
Bentazone
Carbaryl(NAC)
Carbofuran
Carpropamid
Diuron(DCMU)
Dymuron

Fipronil
Flazasulfuron
Halosulfuron-methyl
Iprodione
MBC
Mecoprop(MCPP)
Methomyl
MPP
MPP oxon
MPP oxon sulfone
MPP oxon sulfoxide

MPP sulfone
MPP sulfoxide
Probenazole
Siduron
Simazine(CAT)
Thiobencarb
Thiodicarb
Thiuram
Triclopyr
Tricyclazole

Remarks and Precautions

LabSolutions LCMS Ver. 5.42 SP2 or later is required.
Shimadzu makes no warranty regarding the accuracy of information included in the database or the usefulness of information obtained from using the database.
Be sure to perform tests using standard samples to confirm qualitative and quantitative information obtained with the given system.
To reliably identify registered substances using this database, measure samples using the instrument parameters specified in the method template files included in the product.

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